The synthesis of SBA-Pr-N-Is-Bu-SO3H as a new Hg2+ fluorescent sensor

Ghodsi Mohammadi Ziarani; Shima Roshankar; Fatemeh Mohajer; Alireza Badiei; Mika Sillanpää

doi:10.1016/j.inoche.2022.110100

The synthesis of SBA-Pr-N-Is-Bu-SO₃H as a new Hg²⁺ fluorescent sensor

Ghodsi Mohammadi Ziarani, Shima Roshankar, Fatemeh Mohajer, Alireza Badiei, Mika Sillanpää

Chemical Engineering Technology

Research output: Contribution to journal › Article › peer-review

8 Citations (Scopus)

Abstract

Isatin-based fluorescent chemosensor was synthesized by the treatment of mesoporous SBA-15 with (3-aminopropyl)triethoxysilane, followed by functionalized with isatin and 1,4-butane sultone to achieve SBA-Pr-N-Is-Bu-SO₃H. The compound was tested by FT-IR, EDX, SEM, BET, and TGA techniques. In addition, the fluorescence spectroscopy of the obtained nanomaterial (SBA-Pr-N-Is-Bu-SO₃H) demonstrated that it could be used as a Hg²⁺ ion chemosensor shown high selectivity in aqueous media, and its detection limit was calculated 2.5 × 10⁻⁶ M. It was confirmed an active method for detecting mercury ion selectivity of fluorescence sensors.

Original language	English
Article number	110100
Journal	Inorganic Chemistry Communication
Volume	146
DOIs	https://doi.org/10.1016/j.inoche.2022.110100
Publication status	Published - Dec 2022

Keywords

1,4-Butane sultone
Fluorescent sensor
Mercury ions
SBA-Pr-N-Is-Bu-SOH

ASJC Scopus subject areas

Physical and Theoretical Chemistry
Inorganic Chemistry
Materials Chemistry

Access to Document

10.1016/j.inoche.2022.110100

Cite this

@article{3387303e216a465fa2252331c0aefbb1,

title = "The synthesis of SBA-Pr-N-Is-Bu-SO3H as a new Hg2+ fluorescent sensor",

abstract = "Isatin-based fluorescent chemosensor was synthesized by the treatment of mesoporous SBA-15 with (3-aminopropyl)triethoxysilane, followed by functionalized with isatin and 1,4-butane sultone to achieve SBA-Pr-N-Is-Bu-SO3H. The compound was tested by FT-IR, EDX, SEM, BET, and TGA techniques. In addition, the fluorescence spectroscopy of the obtained nanomaterial (SBA-Pr-N-Is-Bu-SO3H) demonstrated that it could be used as a Hg2+ ion chemosensor shown high selectivity in aqueous media, and its detection limit was calculated 2.5 × 10−6 M. It was confirmed an active method for detecting mercury ion selectivity of fluorescence sensors.",

keywords = "1,4-Butane sultone, Fluorescent sensor, Mercury ions, SBA-Pr-N-Is-Bu-SOH",

author = "{Mohammadi Ziarani}, Ghodsi and Shima Roshankar and Fatemeh Mohajer and Alireza Badiei and Mika Sillanp{\"a}{\"a}",

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year = "2022",

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doi = "10.1016/j.inoche.2022.110100",

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T1 - The synthesis of SBA-Pr-N-Is-Bu-SO3H as a new Hg2+ fluorescent sensor

AU - Mohammadi Ziarani, Ghodsi

AU - Roshankar, Shima

AU - Mohajer, Fatemeh

AU - Badiei, Alireza

AU - Sillanpää, Mika

PY - 2022/12

Y1 - 2022/12

N2 - Isatin-based fluorescent chemosensor was synthesized by the treatment of mesoporous SBA-15 with (3-aminopropyl)triethoxysilane, followed by functionalized with isatin and 1,4-butane sultone to achieve SBA-Pr-N-Is-Bu-SO3H. The compound was tested by FT-IR, EDX, SEM, BET, and TGA techniques. In addition, the fluorescence spectroscopy of the obtained nanomaterial (SBA-Pr-N-Is-Bu-SO3H) demonstrated that it could be used as a Hg2+ ion chemosensor shown high selectivity in aqueous media, and its detection limit was calculated 2.5 × 10−6 M. It was confirmed an active method for detecting mercury ion selectivity of fluorescence sensors.

AB - Isatin-based fluorescent chemosensor was synthesized by the treatment of mesoporous SBA-15 with (3-aminopropyl)triethoxysilane, followed by functionalized with isatin and 1,4-butane sultone to achieve SBA-Pr-N-Is-Bu-SO3H. The compound was tested by FT-IR, EDX, SEM, BET, and TGA techniques. In addition, the fluorescence spectroscopy of the obtained nanomaterial (SBA-Pr-N-Is-Bu-SO3H) demonstrated that it could be used as a Hg2+ ion chemosensor shown high selectivity in aqueous media, and its detection limit was calculated 2.5 × 10−6 M. It was confirmed an active method for detecting mercury ion selectivity of fluorescence sensors.

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KW - Mercury ions

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