Solvothermal synthesis of mesoporous α-GaOOH semi-nanospheres

Manickavachagam Muruganandham; Rominder Suri; Mahmoud S.M. Abdel Wahed; Mika Sillanpää; Bashir Ahmmad; Gang Juan Lee; Jerry J. Wu

doi:10.1016/j.matlet.2013.08.071

Solvothermal synthesis of mesoporous α-GaOOH semi-nanospheres

Manickavachagam Muruganandham
, Rominder Suri
, Mahmoud S.M. Abdel Wahed
, Mika Sillanpää
, Bashir Ahmmad
, Gang Juan Lee
, Jerry J. Wu

Research output: Contribution to journal › Article › peer-review

16 Citations (Scopus)

Abstract

In this letter, we first report on the synthesis of mesoporous α-GaOOH by a solvothermal process. Mesoporous α-GaOOH was synthesized using gallium nitrate in the presence of sodium acetate and ethanol as a solvent at 200 C for 10 h. The synthesized α-GaOOH was characterized using X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM) and nitrogen adsorption analysis. The XRD results showed the formation of well crystallized orthorhombic α-GaOOH. The TEM results showed the formation of semi-nanosphere like morphology. The nitrogen adsorption analysis showed that synthesized α-GaOOH has a very high surface area of 193 m²/g with a narrow pore size distribution of 2.5 nm. The authors propose a plausible mechanism for the formation of α-GaOOH semi-nanospheres.

Original language	English
Pages (from-to)	137-139
Number of pages	3
Journal	Materials Letters
Volume	111
DOIs	https://doi.org/10.1016/j.matlet.2013.08.071
Publication status	Published - 2013
Externally published	Yes

Keywords

Mesoporous materials
Nanocrystalline materials
Structural
α-GaOOH

ASJC Scopus subject areas

General Materials Science
Condensed Matter Physics
Mechanics of Materials
Mechanical Engineering

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10.1016/j.matlet.2013.08.071

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@article{31c988f778974995b7dcfe1be8c6b522,

title = "Solvothermal synthesis of mesoporous α-GaOOH semi-nanospheres",

abstract = "In this letter, we first report on the synthesis of mesoporous α-GaOOH by a solvothermal process. Mesoporous α-GaOOH was synthesized using gallium nitrate in the presence of sodium acetate and ethanol as a solvent at 200 C for 10 h. The synthesized α-GaOOH was characterized using X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM) and nitrogen adsorption analysis. The XRD results showed the formation of well crystallized orthorhombic α-GaOOH. The TEM results showed the formation of semi-nanosphere like morphology. The nitrogen adsorption analysis showed that synthesized α-GaOOH has a very high surface area of 193 m2/g with a narrow pore size distribution of 2.5 nm. The authors propose a plausible mechanism for the formation of α-GaOOH semi-nanospheres.",

keywords = "Mesoporous materials, Nanocrystalline materials, Structural, α-GaOOH",

author = "Manickavachagam Muruganandham and Rominder Suri and \{Abdel Wahed\}, \{Mahmoud S.M.\} and Mika Sillanp{\"a}{\"a} and Bashir Ahmmad and Lee, \{Gang Juan\} and Wu, \{Jerry J.\}",

year = "2013",

doi = "10.1016/j.matlet.2013.08.071",

language = "English",

volume = "111",

pages = "137--139",

journal = "Materials Letters",

issn = "0167-577X",

publisher = "Elsevier B.V.",

}

TY - JOUR

T1 - Solvothermal synthesis of mesoporous α-GaOOH semi-nanospheres

AU - Muruganandham, Manickavachagam

AU - Suri, Rominder

AU - Abdel Wahed, Mahmoud S.M.

AU - Sillanpää, Mika

AU - Ahmmad, Bashir

AU - Lee, Gang Juan

AU - Wu, Jerry J.

PY - 2013

Y1 - 2013

N2 - In this letter, we first report on the synthesis of mesoporous α-GaOOH by a solvothermal process. Mesoporous α-GaOOH was synthesized using gallium nitrate in the presence of sodium acetate and ethanol as a solvent at 200 C for 10 h. The synthesized α-GaOOH was characterized using X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM) and nitrogen adsorption analysis. The XRD results showed the formation of well crystallized orthorhombic α-GaOOH. The TEM results showed the formation of semi-nanosphere like morphology. The nitrogen adsorption analysis showed that synthesized α-GaOOH has a very high surface area of 193 m2/g with a narrow pore size distribution of 2.5 nm. The authors propose a plausible mechanism for the formation of α-GaOOH semi-nanospheres.

AB - In this letter, we first report on the synthesis of mesoporous α-GaOOH by a solvothermal process. Mesoporous α-GaOOH was synthesized using gallium nitrate in the presence of sodium acetate and ethanol as a solvent at 200 C for 10 h. The synthesized α-GaOOH was characterized using X-ray diffraction (XRD), field emission scanning electron microscopy (FE-SEM), transmission electron microscopy (TEM) and nitrogen adsorption analysis. The XRD results showed the formation of well crystallized orthorhombic α-GaOOH. The TEM results showed the formation of semi-nanosphere like morphology. The nitrogen adsorption analysis showed that synthesized α-GaOOH has a very high surface area of 193 m2/g with a narrow pore size distribution of 2.5 nm. The authors propose a plausible mechanism for the formation of α-GaOOH semi-nanospheres.

KW - Mesoporous materials

KW - Nanocrystalline materials

KW - Structural

KW - α-GaOOH

UR - https://www.scopus.com/pages/publications/84883693966

U2 - 10.1016/j.matlet.2013.08.071

DO - 10.1016/j.matlet.2013.08.071

M3 - Article

AN - SCOPUS:84883693966

SN - 0167-577X

VL - 111

SP - 137

EP - 139

JO - Materials Letters

JF - Materials Letters

ER -

Solvothermal synthesis of mesoporous α-GaOOH semi-nanospheres

Abstract

Keywords

ASJC Scopus subject areas

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