Reactive synthesis of CNTs reinforced nickel aluminide composites by spark plasma sintering

Mary A. Awotunde, Adewale O. Adegbenjo, Olusoji O. Ayodele, Avwerosuoghene M. Okoro, Mxolisi B. Shongwe, Peter A. Olubambi

Research output: Contribution to journalArticlepeer-review

10 Citations (Scopus)

Abstract

This work investigated the effect of carbon nanotubes (CNTs) incorporation into the B2 ordered NiAl lattice structure in varying contents, via a unique two stage milling process. The milled powders were consolidated by spark plasma sintering and the sintered composites were extensively characterized using X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), Raman spectroscopy (RS) and nanoindentation techniques. Results show that the NiAl-1.0 wt% CNTs exhibited the best combination of properties with an improved fracture toughness value of 11.25 MPa√m and 306.37 HV for microhardness, while the unreinforced sample showed fracture toughness and microhardness values of 6.93 MPa√m and 349.49 HV respectively. The enhanced fracture toughness was attributed to the retained lengths of the CNTs in addition to the disordering of the ordered lattice structure of NiAl owing to the introduction of the nanotubes.

Original languageEnglish
Article number140070
JournalMaterials Science & Engineering A: Structural Materials: Properties, Microstructure and Processing
Volume796
DOIs
Publication statusPublished - 7 Oct 2020

Keywords

  • Carbon nanotubes
  • Fracture toughness
  • Nanoindentation
  • Nickel aluminide
  • Spark plasma sintering

ASJC Scopus subject areas

  • General Materials Science
  • Condensed Matter Physics
  • Mechanics of Materials
  • Mechanical Engineering

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