Phase selective synthesis of ZnS nanoparticles from structurally new dithiocarbamate precursor

Balasubramaniam Arul Prakasam; Manu Lahtinen; Anssi Peuronen; Manickavachagam Muruganandham; Erkki Kolehmainen; Esa Haapaniemi; Mika Sillanpää

doi:10.1016/j.matlet.2014.12.128

Phase selective synthesis of ZnS nanoparticles from structurally new dithiocarbamate precursor

Balasubramaniam Arul Prakasam, Manu Lahtinen, Anssi Peuronen, Manickavachagam Muruganandham, Erkki Kolehmainen, Esa Haapaniemi, Mika Sillanpää

Research output: Contribution to journal › Article › peer-review

10 Citations (Scopus)

Abstract

A phase selective solvothermal synthesis of ZnS (wurzite) nanoparticles with a flower-like morphology using a dithiocarbamate precursor, [Zn(4-dpmpzdtc)₂(dpmpz)] (1) (where, dpmpz=(diphenylmethyl)piperazine), is described. The nanoparticles were identified as ZnS (wurzite) with the particle size of about 3 to 10 nm by scanning and transmission electron microscopy as well as powder X-ray diffraction (XRD). In addition, the precursor complex 1 was characterized using single crystal X-ray diffraction.

Original language	English
Pages (from-to)	19-21
Number of pages	3
Journal	Materials Letters
Volume	144
DOIs	https://doi.org/10.1016/j.matlet.2014.12.128
Publication status	Published - 1 Apr 2015
Externally published	Yes

Keywords

Crystal structure
Nanoparticles
Solvothermal
Synthesis
Wurzite

ASJC Scopus subject areas

General Materials Science
Condensed Matter Physics
Mechanics of Materials
Mechanical Engineering

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10.1016/j.matlet.2014.12.128

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title = "Phase selective synthesis of ZnS nanoparticles from structurally new dithiocarbamate precursor",

abstract = "A phase selective solvothermal synthesis of ZnS (wurzite) nanoparticles with a flower-like morphology using a dithiocarbamate precursor, [Zn(4-dpmpzdtc)2(dpmpz)] (1) (where, dpmpz=(diphenylmethyl)piperazine), is described. The nanoparticles were identified as ZnS (wurzite) with the particle size of about 3 to 10 nm by scanning and transmission electron microscopy as well as powder X-ray diffraction (XRD). In addition, the precursor complex 1 was characterized using single crystal X-ray diffraction.",

keywords = "Crystal structure, Nanoparticles, Solvothermal, Synthesis, Wurzite",

author = "Prakasam, \{Balasubramaniam Arul\} and Manu Lahtinen and Anssi Peuronen and Manickavachagam Muruganandham and Erkki Kolehmainen and Esa Haapaniemi and Mika Sillanp{\"a}{\"a}",

year = "2015",

month = apr,

day = "1",

doi = "10.1016/j.matlet.2014.12.128",

language = "English",

volume = "144",

pages = "19--21",

journal = "Materials Letters",

issn = "0167-577X",

publisher = "Elsevier B.V.",

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TY - JOUR

T1 - Phase selective synthesis of ZnS nanoparticles from structurally new dithiocarbamate precursor

AU - Prakasam, Balasubramaniam Arul

AU - Lahtinen, Manu

AU - Peuronen, Anssi

AU - Muruganandham, Manickavachagam

AU - Kolehmainen, Erkki

AU - Haapaniemi, Esa

AU - Sillanpää, Mika

PY - 2015/4/1

Y1 - 2015/4/1

N2 - A phase selective solvothermal synthesis of ZnS (wurzite) nanoparticles with a flower-like morphology using a dithiocarbamate precursor, [Zn(4-dpmpzdtc)2(dpmpz)] (1) (where, dpmpz=(diphenylmethyl)piperazine), is described. The nanoparticles were identified as ZnS (wurzite) with the particle size of about 3 to 10 nm by scanning and transmission electron microscopy as well as powder X-ray diffraction (XRD). In addition, the precursor complex 1 was characterized using single crystal X-ray diffraction.

AB - A phase selective solvothermal synthesis of ZnS (wurzite) nanoparticles with a flower-like morphology using a dithiocarbamate precursor, [Zn(4-dpmpzdtc)2(dpmpz)] (1) (where, dpmpz=(diphenylmethyl)piperazine), is described. The nanoparticles were identified as ZnS (wurzite) with the particle size of about 3 to 10 nm by scanning and transmission electron microscopy as well as powder X-ray diffraction (XRD). In addition, the precursor complex 1 was characterized using single crystal X-ray diffraction.

KW - Crystal structure

KW - Nanoparticles

KW - Solvothermal

KW - Synthesis

KW - Wurzite

UR - https://www.scopus.com/pages/publications/84922702298

U2 - 10.1016/j.matlet.2014.12.128

DO - 10.1016/j.matlet.2014.12.128

M3 - Article

AN - SCOPUS:84922702298

SN - 0167-577X

VL - 144

SP - 19

EP - 21

JO - Materials Letters

JF - Materials Letters

ER -

Phase selective synthesis of ZnS nanoparticles from structurally new dithiocarbamate precursor

Abstract

Keywords

ASJC Scopus subject areas

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