Phase selective synthesis of ZnS nanoparticles from structurally new dithiocarbamate precursor

Balasubramaniam Arul Prakasam; Manu Lahtinen; Anssi Peuronen; Manickavachagam Muruganandham; Erkki Kolehmainen; Esa Haapaniemi; Mika Sillanpää

doi:10.1016/j.matlet.2014.12.128

Phase selective synthesis of ZnS nanoparticles from structurally new dithiocarbamate precursor

Balasubramaniam Arul Prakasam, Manu Lahtinen, Anssi Peuronen, Manickavachagam Muruganandham, Erkki Kolehmainen, Esa Haapaniemi, Mika Sillanpää

Research output: Contribution to journal › Article › peer-review

10 Citations (Scopus)

Abstract

A phase selective solvothermal synthesis of ZnS (wurzite) nanoparticles with a flower-like morphology using a dithiocarbamate precursor, [Zn(4-dpmpzdtc)₂(dpmpz)] (1) (where, dpmpz=(diphenylmethyl)piperazine), is described. The nanoparticles were identified as ZnS (wurzite) with the particle size of about 3 to 10 nm by scanning and transmission electron microscopy as well as powder X-ray diffraction (XRD). In addition, the precursor complex 1 was characterized using single crystal X-ray diffraction.

Original language	English
Pages (from-to)	19-21
Number of pages	3
Journal	Materials Letters
Volume	144
DOIs	https://doi.org/10.1016/j.matlet.2014.12.128
Publication status	Published - 1 Apr 2015
Externally published	Yes

Keywords

Crystal structure
Nanoparticles
Solvothermal
Synthesis
Wurzite

ASJC Scopus subject areas

General Materials Science
Condensed Matter Physics
Mechanics of Materials
Mechanical Engineering

Access to Document

10.1016/j.matlet.2014.12.128

Cite this

@article{631c418a65c746debdc25bb29e7ebec6,

title = "Phase selective synthesis of ZnS nanoparticles from structurally new dithiocarbamate precursor",

abstract = "A phase selective solvothermal synthesis of ZnS (wurzite) nanoparticles with a flower-like morphology using a dithiocarbamate precursor, [Zn(4-dpmpzdtc)2(dpmpz)] (1) (where, dpmpz=(diphenylmethyl)piperazine), is described. The nanoparticles were identified as ZnS (wurzite) with the particle size of about 3 to 10 nm by scanning and transmission electron microscopy as well as powder X-ray diffraction (XRD). In addition, the precursor complex 1 was characterized using single crystal X-ray diffraction.",

keywords = "Crystal structure, Nanoparticles, Solvothermal, Synthesis, Wurzite",

author = "Prakasam, {Balasubramaniam Arul} and Manu Lahtinen and Anssi Peuronen and Manickavachagam Muruganandham and Erkki Kolehmainen and Esa Haapaniemi and Mika Sillanp{\"a}{\"a}",

year = "2015",

month = apr,

day = "1",

doi = "10.1016/j.matlet.2014.12.128",

language = "English",

volume = "144",

pages = "19--21",

journal = "Materials Letters",

issn = "0167-577X",

publisher = "Elsevier",

}

TY - JOUR

T1 - Phase selective synthesis of ZnS nanoparticles from structurally new dithiocarbamate precursor

AU - Prakasam, Balasubramaniam Arul

AU - Lahtinen, Manu

AU - Peuronen, Anssi

AU - Muruganandham, Manickavachagam

AU - Kolehmainen, Erkki

AU - Haapaniemi, Esa

AU - Sillanpää, Mika

PY - 2015/4/1

Y1 - 2015/4/1

N2 - A phase selective solvothermal synthesis of ZnS (wurzite) nanoparticles with a flower-like morphology using a dithiocarbamate precursor, [Zn(4-dpmpzdtc)2(dpmpz)] (1) (where, dpmpz=(diphenylmethyl)piperazine), is described. The nanoparticles were identified as ZnS (wurzite) with the particle size of about 3 to 10 nm by scanning and transmission electron microscopy as well as powder X-ray diffraction (XRD). In addition, the precursor complex 1 was characterized using single crystal X-ray diffraction.

AB - A phase selective solvothermal synthesis of ZnS (wurzite) nanoparticles with a flower-like morphology using a dithiocarbamate precursor, [Zn(4-dpmpzdtc)2(dpmpz)] (1) (where, dpmpz=(diphenylmethyl)piperazine), is described. The nanoparticles were identified as ZnS (wurzite) with the particle size of about 3 to 10 nm by scanning and transmission electron microscopy as well as powder X-ray diffraction (XRD). In addition, the precursor complex 1 was characterized using single crystal X-ray diffraction.

KW - Crystal structure

KW - Nanoparticles

KW - Solvothermal

KW - Synthesis

KW - Wurzite

UR - http://www.scopus.com/inward/record.url?scp=84922702298&partnerID=8YFLogxK

U2 - 10.1016/j.matlet.2014.12.128

DO - 10.1016/j.matlet.2014.12.128

M3 - Article

AN - SCOPUS:84922702298

SN - 0167-577X

VL - 144

SP - 19

EP - 21

JO - Materials Letters

JF - Materials Letters

ER -

Phase selective synthesis of ZnS nanoparticles from structurally new dithiocarbamate precursor

Abstract

Keywords

ASJC Scopus subject areas

Access to Document

Other files and links

Fingerprint

Cite this