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Morphology and Mechanical Properties of Star Block Copolymer Modified Epoxy Resin Blends

  • Shankar P. Khatiwada
  • , C. Sarath Chandran
  • , Ralf Lach
  • , Marco Liebscher
  • , Jean Marc Saiter
  • , Sabu Thomas
  • , Gert Heinrich
  • , Rameshwar Adhikari
  • Tribhuvan University
  • Leibniz Institute of Polymer Research Dresden
  • Mahatma Gandhi University, Kottayam
  • Polymer Service GmbH
  • Université de Rouen-Laboratoire ECODIV

Research output: Contribution to journalConference articlepeer-review

9 Citations (Scopus)

Abstract

In this work, we investigate the morphological and mechanical properties of blends of diglycidyl ether of bisphenol-A (DGEBA) and epoxidized polystyrene-polybutadiene star block copolymer (epST3) using diamino-diphenyl sulphone (DDS) as a hardener. The epoxidation of the star block copolymer was performed using meta-chloroperoxybenzoic acid (m-CPBA). Chemical modification of the copolymer was characterized by Fourier transform infrared (FTIR) spectroscopy while the morphology of the blends was analyzed by microscopic techniques. The mechanical behavior of the blends was analyzed by recording microindentation as well as impact tests. It has been demonstrated that the completely macrophase-separated morphology of the blends could be dispersed into the structures comprising co-continuous networks of the block copolymer phase and the epoxy resin leading to an increment in impact strength. At the same time, the hardness and stiffness of the blends, as shown by the indentation microhardness and indentation modulus, was maintained to a pretty high level.

Original languageEnglish
Pages (from-to)5734-5742
Number of pages9
JournalMaterials Today: Proceedings
Volume4
Issue number4
DOIs
Publication statusPublished - 2017
Externally publishedYes
Event2016 International Conference on Multifunctional Materials for Device Applications, ICMDA 2016 - Patna, India
Duration: 26 Oct 201628 Oct 2016

Keywords

  • block copolymer
  • electron microscopy
  • epoxy resin
  • impact strength
  • mechanical properties
  • morphology

ASJC Scopus subject areas

  • General Materials Science

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