Facile fabrication of flower like self-assembled mesoporous hierarchical microarchitectures of In(OH)3 and In2O3: In(OH)3 micro flowers with electron beam sensitive thin petals

Balasubramaniam Arul Prakasam; Manu Lahtinen; Anssi Peuronen; Manickavachagam Muruganandham; Mika Sillanpää

doi:10.1016/j.matchemphys.2016.09.040

Facile fabrication of flower like self-assembled mesoporous hierarchical microarchitectures of In(OH)₃ and In₂O₃: In(OH)₃ micro flowers with electron beam sensitive thin petals

Balasubramaniam Arul Prakasam
, Manu Lahtinen
, Anssi Peuronen
, Manickavachagam Muruganandham
, Mika Sillanpää

Research output: Contribution to journal › Article › peer-review

5 Citations (Scopus)

Abstract

A template and capping-reagent free facile fabrication method for mesoporous hierarchical microarchitectures of flower-like In(OH)₃ particles under benign hydrothermal conditions is reported. Calcination of In(OH)₃ to In₂O₃ with the retention of morphology is also described. Both In(OH)₃ and In₂O₃ microstructures were analyzed with SEM, EDX, TEM and powder X-ray diffraction. The crystal sizes for In(OH)₃ and In₂O₃ were calculated using the Scherrer equation. In In(OH)₃ the thin flakes at the periphery of micro flowers were electron beam sensitive. The mechanism of self-assembly process was analyzed as well.

Original language	English
Pages (from-to)	183-188
Number of pages	6
Journal	Materials Chemistry and Physics
Volume	184
DOIs	https://doi.org/10.1016/j.matchemphys.2016.09.040
Publication status	Published - 1 Dec 2016
Externally published	Yes

Keywords

Microporous materials
Microstructure
Oxides
Semiconductors

ASJC Scopus subject areas

General Materials Science
Condensed Matter Physics

Access to Document

10.1016/j.matchemphys.2016.09.040

Cite this

@article{347e839a72e84302ad87f26615e2c1de,

title = "Facile fabrication of flower like self-assembled mesoporous hierarchical microarchitectures of In(OH)3 and In2O3: In(OH)3 micro flowers with electron beam sensitive thin petals",

abstract = "A template and capping-reagent free facile fabrication method for mesoporous hierarchical microarchitectures of flower-like In(OH)3 particles under benign hydrothermal conditions is reported. Calcination of In(OH)3 to In2O3 with the retention of morphology is also described. Both In(OH)3 and In2O3 microstructures were analyzed with SEM, EDX, TEM and powder X-ray diffraction. The crystal sizes for In(OH)3 and In2O3 were calculated using the Scherrer equation. In In(OH)3 the thin flakes at the periphery of micro flowers were electron beam sensitive. The mechanism of self-assembly process was analyzed as well.",

keywords = "Microporous materials, Microstructure, Oxides, Semiconductors",

author = "\{Arul Prakasam\}, Balasubramaniam and Manu Lahtinen and Anssi Peuronen and Manickavachagam Muruganandham and Mika Sillanp{\"a}{\"a}",

note = "Publisher Copyright: {\textcopyright} 2016 Elsevier B.V.",

year = "2016",

month = dec,

day = "1",

doi = "10.1016/j.matchemphys.2016.09.040",

language = "English",

volume = "184",

pages = "183--188",

journal = "Materials Chemistry and Physics",

issn = "0254-0584",

publisher = "Elsevier B.V.",

}

Facile fabrication of flower like self-assembled mesoporous hierarchical microarchitectures of In(OH)₃ and In₂O₃: In(OH)₃ micro flowers with electron beam sensitive thin petals. / Arul Prakasam, Balasubramaniam; Lahtinen, Manu; Peuronen, Anssi et al.
In: Materials Chemistry and Physics, Vol. 184, 01.12.2016, p. 183-188.

Research output: Contribution to journal › Article › peer-review

TY - JOUR

T1 - Facile fabrication of flower like self-assembled mesoporous hierarchical microarchitectures of In(OH)3 and In2O3

T2 - In(OH)3 micro flowers with electron beam sensitive thin petals

AU - Arul Prakasam, Balasubramaniam

AU - Lahtinen, Manu

AU - Peuronen, Anssi

AU - Muruganandham, Manickavachagam

AU - Sillanpää, Mika

PY - 2016/12/1

Y1 - 2016/12/1

N2 - A template and capping-reagent free facile fabrication method for mesoporous hierarchical microarchitectures of flower-like In(OH)3 particles under benign hydrothermal conditions is reported. Calcination of In(OH)3 to In2O3 with the retention of morphology is also described. Both In(OH)3 and In2O3 microstructures were analyzed with SEM, EDX, TEM and powder X-ray diffraction. The crystal sizes for In(OH)3 and In2O3 were calculated using the Scherrer equation. In In(OH)3 the thin flakes at the periphery of micro flowers were electron beam sensitive. The mechanism of self-assembly process was analyzed as well.

AB - A template and capping-reagent free facile fabrication method for mesoporous hierarchical microarchitectures of flower-like In(OH)3 particles under benign hydrothermal conditions is reported. Calcination of In(OH)3 to In2O3 with the retention of morphology is also described. Both In(OH)3 and In2O3 microstructures were analyzed with SEM, EDX, TEM and powder X-ray diffraction. The crystal sizes for In(OH)3 and In2O3 were calculated using the Scherrer equation. In In(OH)3 the thin flakes at the periphery of micro flowers were electron beam sensitive. The mechanism of self-assembly process was analyzed as well.

KW - Microporous materials

KW - Microstructure

KW - Oxides

KW - Semiconductors

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U2 - 10.1016/j.matchemphys.2016.09.040

DO - 10.1016/j.matchemphys.2016.09.040

M3 - Article

AN - SCOPUS:84994454861

SN - 0254-0584

VL - 184

SP - 183

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JO - Materials Chemistry and Physics

JF - Materials Chemistry and Physics

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