Effect of flow velocity on corrosion behaviour of spark plasma sintered Fe-Cr-Ni reinforced with TiN in 3.5 wt% NaCl

O. O. Ige; S. R. Oke; O. E. Falodun; S. Aribo; K. M. Oluwasegun; O. O. Ajibola; J. O. Olawale; A. Ogunbadejo; O. T. Olalemi; P. A. Olubambi

doi:10.1016/j.matpr.2020.03.709

Effect of flow velocity on corrosion behaviour of spark plasma sintered Fe-Cr-Ni reinforced with TiN in 3.5 wt% NaCl

O. O. Ige, S. R. Oke, O. E. Falodun, S. Aribo, K. M. Oluwasegun, O. O. Ajibola, J. O. Olawale, A. Ogunbadejo, O. T. Olalemi, P. A. Olubambi

Metallurgy

Research output: Contribution to journal › Conference article › peer-review

3 Citations (Scopus)

Abstract

This study investigated the effect of varying flow velocities on the corrosion behavior of titanium nitride reinforced Fe-Cr-Ni (Duplex Stainless Steel - UNS S32205) manufactured by spark plasma sintering. The TiN reinforcement was within the range of 0-8% at an interval of 2%. The spark plasma sintering parameters are sintering temperature (1150 °C), sintering time (10 mins), applied pressure (50 Mpa) and heating rate (100 °C/mins). The sintered samples were subjected to both gravimetric and electrochemical measurement in 3.5 wt% NaCl at a flow velocity of 1.0 m/s and increasing at 0.5 m/s till 2.5 m/s. A field emission scanning electron microscope (FESEM) equipped with energy dispersive x-ray spectrometer (EDS) was employed to carry out the microstructural characterizations of the corroded sintered products. The results showed that increasing the flow velocity decreased the passive current, but leads to more positive corrosion potential of the sintered products. The active-passive behaviour and the role of microstructures on the reinforced sintered composites in 3.5 wt% NaCl are discussed.

Original language	English
Pages (from-to)	688-695
Number of pages	8
Journal	Materials Today: Proceedings
Volume	38
DOIs	https://doi.org/10.1016/j.matpr.2020.03.709
Publication status	Published - 1 Jan 2021
Event	2020 International Symposium on Nanostructured, Nanoengineered and Advanced Materials, ISNNAM 2020 - Gold Reef City, South Africa Duration: 30 Apr 2020 → 3 May 2020

Keywords

DSS 2205
Flow induced-corrosion
Powders
Simulated seawater
Sintering
Titanium nitride

ASJC Scopus subject areas

General Materials Science

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10.1016/j.matpr.2020.03.709

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@article{46582cdef5cd4b79b8a0d0399b89db8c,

title = "Effect of flow velocity on corrosion behaviour of spark plasma sintered Fe-Cr-Ni reinforced with TiN in 3.5 wt% NaCl",

abstract = "This study investigated the effect of varying flow velocities on the corrosion behavior of titanium nitride reinforced Fe-Cr-Ni (Duplex Stainless Steel - UNS S32205) manufactured by spark plasma sintering. The TiN reinforcement was within the range of 0-8% at an interval of 2%. The spark plasma sintering parameters are sintering temperature (1150 °C), sintering time (10 mins), applied pressure (50 Mpa) and heating rate (100 °C/mins). The sintered samples were subjected to both gravimetric and electrochemical measurement in 3.5 wt% NaCl at a flow velocity of 1.0 m/s and increasing at 0.5 m/s till 2.5 m/s. A field emission scanning electron microscope (FESEM) equipped with energy dispersive x-ray spectrometer (EDS) was employed to carry out the microstructural characterizations of the corroded sintered products. The results showed that increasing the flow velocity decreased the passive current, but leads to more positive corrosion potential of the sintered products. The active-passive behaviour and the role of microstructures on the reinforced sintered composites in 3.5 wt% NaCl are discussed.",

keywords = "DSS 2205, Flow induced-corrosion, Powders, Simulated seawater, Sintering, Titanium nitride",

author = "Ige, {O. O.} and Oke, {S. R.} and Falodun, {O. E.} and S. Aribo and Oluwasegun, {K. M.} and Ajibola, {O. O.} and Olawale, {J. O.} and A. Ogunbadejo and Olalemi, {O. T.} and Olubambi, {P. A.}",

note = "Publisher Copyright: {\textcopyright} 2019 Elsevier Ltd. All rights reserved. Selection and peer-review under responsibility of the scientific committee of the International Symposium on Nanostructured, Nanoengineered and Advanced Materials.; 2020 International Symposium on Nanostructured, Nanoengineered and Advanced Materials, ISNNAM 2020 ; Conference date: 30-04-2020 Through 03-05-2020",

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doi = "10.1016/j.matpr.2020.03.709",

language = "English",

volume = "38",

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journal = "Materials Today: Proceedings",

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TY - JOUR

T1 - Effect of flow velocity on corrosion behaviour of spark plasma sintered Fe-Cr-Ni reinforced with TiN in 3.5 wt% NaCl

AU - Ige, O. O.

AU - Oke, S. R.

AU - Falodun, O. E.

AU - Aribo, S.

AU - Oluwasegun, K. M.

AU - Ajibola, O. O.

AU - Olawale, J. O.

AU - Ogunbadejo, A.

AU - Olalemi, O. T.

AU - Olubambi, P. A.

N1 - Publisher Copyright: © 2019 Elsevier Ltd. All rights reserved. Selection and peer-review under responsibility of the scientific committee of the International Symposium on Nanostructured, Nanoengineered and Advanced Materials.

PY - 2021/1/1

Y1 - 2021/1/1

N2 - This study investigated the effect of varying flow velocities on the corrosion behavior of titanium nitride reinforced Fe-Cr-Ni (Duplex Stainless Steel - UNS S32205) manufactured by spark plasma sintering. The TiN reinforcement was within the range of 0-8% at an interval of 2%. The spark plasma sintering parameters are sintering temperature (1150 °C), sintering time (10 mins), applied pressure (50 Mpa) and heating rate (100 °C/mins). The sintered samples were subjected to both gravimetric and electrochemical measurement in 3.5 wt% NaCl at a flow velocity of 1.0 m/s and increasing at 0.5 m/s till 2.5 m/s. A field emission scanning electron microscope (FESEM) equipped with energy dispersive x-ray spectrometer (EDS) was employed to carry out the microstructural characterizations of the corroded sintered products. The results showed that increasing the flow velocity decreased the passive current, but leads to more positive corrosion potential of the sintered products. The active-passive behaviour and the role of microstructures on the reinforced sintered composites in 3.5 wt% NaCl are discussed.

AB - This study investigated the effect of varying flow velocities on the corrosion behavior of titanium nitride reinforced Fe-Cr-Ni (Duplex Stainless Steel - UNS S32205) manufactured by spark plasma sintering. The TiN reinforcement was within the range of 0-8% at an interval of 2%. The spark plasma sintering parameters are sintering temperature (1150 °C), sintering time (10 mins), applied pressure (50 Mpa) and heating rate (100 °C/mins). The sintered samples were subjected to both gravimetric and electrochemical measurement in 3.5 wt% NaCl at a flow velocity of 1.0 m/s and increasing at 0.5 m/s till 2.5 m/s. A field emission scanning electron microscope (FESEM) equipped with energy dispersive x-ray spectrometer (EDS) was employed to carry out the microstructural characterizations of the corroded sintered products. The results showed that increasing the flow velocity decreased the passive current, but leads to more positive corrosion potential of the sintered products. The active-passive behaviour and the role of microstructures on the reinforced sintered composites in 3.5 wt% NaCl are discussed.

KW - DSS 2205

KW - Flow induced-corrosion

KW - Powders

KW - Simulated seawater

KW - Sintering

KW - Titanium nitride

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U2 - 10.1016/j.matpr.2020.03.709

DO - 10.1016/j.matpr.2020.03.709

M3 - Conference article

AN - SCOPUS:85104301543

SN - 2214-7853

VL - 38

SP - 688

EP - 695

JO - Materials Today: Proceedings

JF - Materials Today: Proceedings

T2 - 2020 International Symposium on Nanostructured, Nanoengineered and Advanced Materials, ISNNAM 2020

Y2 - 30 April 2020 through 3 May 2020

ER -

Effect of flow velocity on corrosion behaviour of spark plasma sintered Fe-Cr-Ni reinforced with TiN in 3.5 wt% NaCl

Abstract

Keywords

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