Detailed example of the identification and crystallographic analysis of a pseudo-merohedrally twinned crystal

Ilia Guzei; Regine Herbst-Irmer; Apollinaire Munyaneza; James Darkwa

doi:10.1107/S0108768112002728

Detailed example of the identification and crystallographic analysis of a pseudo-merohedrally twinned crystal

Ilia Guzei, Regine Herbst-Irmer, Apollinaire Munyaneza, James Darkwa

Chemical Sciences

Research output: Contribution to journal › Article › peer-review

7 Citations (Scopus)

Abstract

A detailed description of the procedures utilized in the non-routine X-ray single-crystal structural determination and refinement of a pseudo-merohedrally twinned crystal of an Fe/Ni organometallic complex is presented. It illustrates to the practitioners of crystallography how to properly handle such cases and describes the logic and concrete steps necessary to account for the twinning, pseudo-symmetry and atomic positional disorder.

Original language	English
Pages (from-to)	150-157
Number of pages	8
Journal	Acta Crystallographica Section B: Structural Science
Volume	68
Issue number	2
DOIs	https://doi.org/10.1107/S0108768112002728
Publication status	Published - Apr 2012

Keywords

pseudo-symmetry
twinning

ASJC Scopus subject areas

General Biochemistry,Genetics and Molecular Biology

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Detailed example of the identification and crystallographic analysis of a pseudo-merohedrally twinned crystal

Abstract

Keywords

ASJC Scopus subject areas

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