Crystallite size determination of thermally deposited Gold Nanoparticles

Olasupo Daniel Ogundare; Ojo Jeremiah Akinribide; Adelana Rasak Adetunji; Mosobalaje Oyebanji Adeoye; Peter Apata Olubambi

doi:10.1016/j.promfg.2019.02.025

Crystallite size determination of thermally deposited Gold Nanoparticles

Olasupo Daniel Ogundare, Ojo Jeremiah Akinribide, Adelana Rasak Adetunji, Mosobalaje Oyebanji Adeoye, Peter Apata Olubambi

Metallurgy

Research output: Contribution to journal › Conference article › peer-review

20 Citations (Scopus)

Abstract

This paper has x-rayed an approach to investigate the crystallite size of thermally deposited gold nanoparticles on a glass substrate. The mined and beneficiated gold sample was deposited on glass slide in Nano-38 thermal depositor after the substrate has been technically prepared. The crystallite size and profile fitting of the nanoparticles were determined by X-ray Diffractometer (XRD). The result showed that the average crystallite size of Au nanoparticles thermally deposited on glass slide was 14.4 ± 6.7 nm with lattice constants: a, b, c; 4.0789, 4.0789, and 4.0789 (Å) respectively. The TEM images have confirmed that high quality spherical Au NPs that were between 18 nm - 24 nm were successfully synthesized. The XRD has shown that the material of the gold nanoparticles is gold and crystalline in structure. Narrow size distribution and small monosize gold nanoparticles produced may proffer advantages for self-assembled monolayer formation and enhanced surface area.

Original language	English
Pages (from-to)	173-179
Number of pages	7
Journal	Procedia Manufacturing
Volume	30
DOIs	https://doi.org/10.1016/j.promfg.2019.02.025
Publication status	Published - 2019
Event	14th Global Congress on Manufacturing and Management, GCMM 2018 - Brisbane, Australia Duration: 5 Dec 2018 → 7 Dec 2018

Keywords

Crystallite size
Gold nanoparticles
Thermal deposition
XRD

ASJC Scopus subject areas

Industrial and Manufacturing Engineering
Artificial Intelligence

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10.1016/j.promfg.2019.02.025

Cite this

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title = "Crystallite size determination of thermally deposited Gold Nanoparticles",

abstract = "This paper has x-rayed an approach to investigate the crystallite size of thermally deposited gold nanoparticles on a glass substrate. The mined and beneficiated gold sample was deposited on glass slide in Nano-38 thermal depositor after the substrate has been technically prepared. The crystallite size and profile fitting of the nanoparticles were determined by X-ray Diffractometer (XRD). The result showed that the average crystallite size of Au nanoparticles thermally deposited on glass slide was 14.4 ± 6.7 nm with lattice constants: a, b, c; 4.0789, 4.0789, and 4.0789 ({\AA}) respectively. The TEM images have confirmed that high quality spherical Au NPs that were between 18 nm - 24 nm were successfully synthesized. The XRD has shown that the material of the gold nanoparticles is gold and crystalline in structure. Narrow size distribution and small monosize gold nanoparticles produced may proffer advantages for self-assembled monolayer formation and enhanced surface area.",

keywords = "Crystallite size, Gold nanoparticles, Thermal deposition, XRD",

author = "Ogundare, {Olasupo Daniel} and Akinribide, {Ojo Jeremiah} and Adetunji, {Adelana Rasak} and Adeoye, {Mosobalaje Oyebanji} and Olubambi, {Peter Apata}",

note = "Publisher Copyright: {\textcopyright} 2019 The Authors. Published by Elsevier Ltd.; 14th Global Congress on Manufacturing and Management, GCMM 2018 ; Conference date: 05-12-2018 Through 07-12-2018",

year = "2019",

doi = "10.1016/j.promfg.2019.02.025",

language = "English",

volume = "30",

pages = "173--179",

journal = "Procedia Manufacturing",

issn = "2351-9789",

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TY - JOUR

T1 - Crystallite size determination of thermally deposited Gold Nanoparticles

AU - Ogundare, Olasupo Daniel

AU - Akinribide, Ojo Jeremiah

AU - Adetunji, Adelana Rasak

AU - Adeoye, Mosobalaje Oyebanji

AU - Olubambi, Peter Apata

PY - 2019

Y1 - 2019

N2 - This paper has x-rayed an approach to investigate the crystallite size of thermally deposited gold nanoparticles on a glass substrate. The mined and beneficiated gold sample was deposited on glass slide in Nano-38 thermal depositor after the substrate has been technically prepared. The crystallite size and profile fitting of the nanoparticles were determined by X-ray Diffractometer (XRD). The result showed that the average crystallite size of Au nanoparticles thermally deposited on glass slide was 14.4 ± 6.7 nm with lattice constants: a, b, c; 4.0789, 4.0789, and 4.0789 (Å) respectively. The TEM images have confirmed that high quality spherical Au NPs that were between 18 nm - 24 nm were successfully synthesized. The XRD has shown that the material of the gold nanoparticles is gold and crystalline in structure. Narrow size distribution and small monosize gold nanoparticles produced may proffer advantages for self-assembled monolayer formation and enhanced surface area.

AB - This paper has x-rayed an approach to investigate the crystallite size of thermally deposited gold nanoparticles on a glass substrate. The mined and beneficiated gold sample was deposited on glass slide in Nano-38 thermal depositor after the substrate has been technically prepared. The crystallite size and profile fitting of the nanoparticles were determined by X-ray Diffractometer (XRD). The result showed that the average crystallite size of Au nanoparticles thermally deposited on glass slide was 14.4 ± 6.7 nm with lattice constants: a, b, c; 4.0789, 4.0789, and 4.0789 (Å) respectively. The TEM images have confirmed that high quality spherical Au NPs that were between 18 nm - 24 nm were successfully synthesized. The XRD has shown that the material of the gold nanoparticles is gold and crystalline in structure. Narrow size distribution and small monosize gold nanoparticles produced may proffer advantages for self-assembled monolayer formation and enhanced surface area.

KW - Crystallite size

KW - Gold nanoparticles

KW - Thermal deposition

KW - XRD

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U2 - 10.1016/j.promfg.2019.02.025

DO - 10.1016/j.promfg.2019.02.025

M3 - Conference article

AN - SCOPUS:85067289908

SN - 2351-9789

VL - 30

SP - 173

EP - 179

JO - Procedia Manufacturing

JF - Procedia Manufacturing

T2 - 14th Global Congress on Manufacturing and Management, GCMM 2018

Y2 - 5 December 2018 through 7 December 2018

ER -

Crystallite size determination of thermally deposited Gold Nanoparticles

Abstract

Keywords

ASJC Scopus subject areas

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